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    • Home
    • About
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+1.800 215 2629

  • Home
  • About
  • GC-HRMS
  • GDMS- Magnetic Sector
  • Glow Discharge GD-MSQ
  • LA-ICPMS
  • LC-ICPMS
  • ICP-MS
  • Contact
Mass Spectrometry instruments for organic and inorganic analysis.

Glow Discharge Mass Spectrometry

About MSI - Mass Spec Instruments for elemental, molecular & isotopes

 The GD90 is a Glow Discharge HR high resolution MS offering direct elemental analysis (matrix to ultra-trace) in a variety of materials.  

Glow discharge occurs on a molecular level by applying a potential difference between the anode and the cathode (analyte). As atomization and ionization occur separately, minimal matrix effects are observed. This makes it possible to use a standard Relative Sensitivity Factors (RSF) data set for all analyses.

After atomization and ionization in the plasma, the ions (M+) diffuse outside the cell and are accelerated down the flight path, through the electrostatic analyzer (ESA) and the magnetic analyzer (the magnet) to increase ion separation before detection by either the electron multiplier or Faraday cup, depending on signal intensity. 

Reliable Scientific Equipment for Your Lab

Advantages of GDMS

Features of the GD90 Trace

Features of the GD90 Trace

  • Full elemental analysis of major (wt. %) to ultra-trace elements (ppb to sub-ppb) within a single scan
  • Direct solid sampling technique, thus alleviating the need for chemical digestion
  • Continuously variable high resolution capabilities from <400 to >10,000 RP (10% valley definition)
  • Dual collectors allowing up to 12 orders of linear dynamic range
  • A proven technique for high sensitivity depth-dependent distribution analysis of trace elements in coatings and other multi-layered advanced materials
  • Minimal matrix effects allow calibration without matrix matched standards by using Relative Sensitivity Factors (RSF)

Features of the GD90 Trace

Features of the GD90 Trace

Features of the GD90 Trace

  • Tantalum cell and source construction for ease of cleaning
  • Availability of cryo-cooling of the GD cell to minimise gas backgrounds
  • Accommodates both pin and flat cell geometries
  • No mass bias for light/heavy elements
  • Calibration consists of a quick check of 180Ta and 181Ta to ensure that the IC and Faraday detectors are in agreement
  • Low gas flow allows for cost-effective use of an alternate ionisation gas such as krypton
  • Ability to analyse a wide range of samples ranging from alloys to high purity materials (both conductive and non-conductive), in a plethora of sample geometries
  • Low sputter rate – at normal analytical conditions the sputter rate ranges from 150 nm/minute (conductive) to 100 nm/minute (non-conductive); lowering operational conditions allows sputter rate to be slowed by at least 5x
  • RSFs and Detection Limit determinations are derived from published, readily sourced methods
  • Front end assembly allows for the fitting of a custom-designed glove box for nuclear applications

Spectrometer Experts USA

Features of the GD90 Trace

Spectrometer Experts USA

  • To meet the ever-growing needs for GDMS, MSI is proud to employ a team of highly skilled dedicated GDMS personnel with over 35 years of combined GDMS experience. 
  • This GDMS expertise allows for instrumental and applications development, as well as thorough operational and analytical training specific for each customer. 

Contact Us

MSI - Mass Spectrometry Instruments

1930 Dunbar Rd, Cayce, SC 29033, USA

+1.800 215 2629 bjohns@MSInstruments.us

Hours

Mon

09:00 am – 05:00 pm

Tue

09:00 am – 05:00 pm

Wed

09:00 am – 05:00 pm

Thu

09:00 am – 05:00 pm

Fri

09:00 am – 05:00 pm

Sat

Closed

Sun

Closed

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  • About
  • GC-HRMS
  • GDMS- Magnetic Sector
  • Glow Discharge GD-MSQ
  • LA-ICPMS
  • LC-ICPMS
  • ICP-MS
  • Contact

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